در هنگام جستجو کلمه در قسمت عنوان میتوانید کلمات مورد جستجو را با کاراکتر (-) جدا کنید.
کاربرد نوع شرط:
- جایگاه : پژوهشی
- مجله: Asian Journal of Green Chemistry
- نوع مقاله: Journal Article
- کلمات کلیدی: Surface morphology,Electrolysis,Organic electro-synthesis,cathode
- چکیده:
- چکیده انگلیسی: This paper presents an innovative, green and organic electro synthesis in order to prepare Schiff base product by the reduction of 5-methoxy-5,6-bis (3-nitropheyl-4,5-dihydro-1,2,4-triazine-3(2H))-thione followed by the condensation on zinc cathode in aqueous alkaline ethanol media in the presence of salicylaldehyde at room temperature. The main characteristic of this proposal is the electro-reduction and electro-condensation. The bulk electrolysis at constant potential was performed in a three-electrode undivided cell in order to prepare Schiff base. In this sense, good yields and easy purification were achieved. Results indicate that thereduction produced high current in the cell and succeeded a green chemistry process. Products were characterized by IR, NMR (1H, 13C), and SEM.
- انتشار مقاله: 01-11-1397
- نویسندگان: Sasigolli Annappa Srikanta,Putta Naik Parmeswara Naik,Ganga Naik Krishanamurthy
- مشاهده